3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

Base Information

Chemical Name:3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate
CAS No.:1263862-40-3
Molecular Formula:BF₄*C₂₁H₂₆N₃
Molecular Weight:407.262
Hs Code.:

Synonyms:3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

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Chemical Property of 3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

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Technology Process of 3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

There total 4 articles about 3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1251555-83-5
1,4-bis(2,4,6-trimethylphenyl)-1H-[1,2,3]-triazole

: 420-37-1
trimethoxonium tetrafluoroborate

: 1263862-40-3
3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

Guidance literature:: In dichloromethane; at 20 ℃; for 16h; Schlenk technique; Inert atmosphere;
DOI:10.1039/C8CC05309J

Reference yield:

: 14213-00-4
2,4,6-trimethylaniline azide

: 769-26-6
2-ethynyl-1,3,5-trimethylbenzene

: 1263862-40-3
3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) sulfate; sodium L-ascorbate

2: dichloromethane / 48 h / Inert atmosphere

With copper(II) sulfate; sodium L-ascorbate; In dichloromethane;
DOI:10.1002/ejic.201101383

Reference yield:

: 769-26-6
2-ethynyl-1,3,5-trimethylbenzene

: 1263862-40-3
3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / tert-butyl alcohol; water / 16 h / 25 °C / Schlenk technique

2: dichloromethane / 16 h / 20 °C / Schlenk technique; Inert atmosphere

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; tert-butyl alcohol;
DOI:10.1039/C8CC05309J