5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

Base Information

Chemical Name:5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline
CAS No.:947590-18-3
Molecular Formula:C₁₂H₈Cl₂N₂O
Molecular Weight:267.114
Hs Code.:

Synonyms:5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

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Technology Process of 5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

There total 4 articles about 5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 106-47-8
4-chloro-aniline

: 100-00-5
4-chlorobenzonitrile

: 947590-18-3
5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

Guidance literature:: 4-chloro-aniline; With potassium tert-butylate; In N,N-dimethyl-formamide; at -60 ℃; for 0.0833333h;

4-chlorobenzonitrile; In N,N-dimethyl-formamide; for 0.5h;
DOI:10.1002/ejoc.201900526

Reference yield:

: C₁₂H₉N₂Cl₂O₂^(1-)

: 947590-18-3
5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

Guidance literature:: With acetic acid; In N,N-dimethyl-formamide;
DOI:10.1055/s-2007-982534

Reference yield:

: 106-47-8
4-chloro-aniline

: 947590-18-3
5-chloro-N-(4-chlorophenyl)-2-nitrosoaniline

Guidance literature:: Multi-step reaction with 2 steps

1: t-BuOK / dimethylformamide / -60 °C

2: AcOH / dimethylformamide

With potassium tert-butylate; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1055/s-2007-982534