6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Base Information

Chemical Name:6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine
CAS No.:956235-21-5
Molecular Formula:C₂₁H₃₆N₂O₃S
Molecular Weight:396.594
Hs Code.:

Synonyms:6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

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Chemical Property of 6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

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Technology Process of 6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

There total 14 articles about 6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.6%

: 956235-20-4
2-(6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexyl)-1H-isoindole-1,3(2H)-dione

: 956235-21-5
6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: With hydrazine; In ethanol; at 20 ℃; for 86h; Heating / reflux;

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 956235-21-5
6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / tetrabutylammomium bromide / water / 5 h / 20 °C

2: cetyltributylphosphonium bromide / N,N-dimethyl-formamide / 3 h / 75 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 20 °C / 2070.21 Torr

4: triethylamine / dichloromethane / 20 °C

5: sodium hydrogencarbonate / N,N-dimethyl-formamide / 22 h / 70 °C

6: hydrazine / ethanol / 86 h / 20 °C / Heating / reflux

With sodium hydroxide; hydrogen; sodium hydrogencarbonate; triethylamine; hydrazine; palladium 10% on activated carbon; tetrabutylammomium bromide; cetyltributylphosphonium bromide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 956235-14-6
methyl 3-(cyclopentylthio)benzoate

: 956235-21-5
6-{2-[[3-(cyclopentylsulfonyl)benzyl](methyl)amino]ethoxy}hexan-1-amine

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 64 h / 0 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran / 16 h / 20 °C

2.2: pH 3

3.1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 2.25 h / 0 - 20 °C

4.1: tetrahydrofuran / 16 h / -30 - 20 °C

5.1: borane-THF / tetrahydrofuran / 20 °C / Heating / reflux

5.3: 0.5 h

6.1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 22 h / 70 °C

7.1: hydrazine / ethanol / 86 h / 20 °C / Heating / reflux

With lithium hydroxide; borane-THF; oxalyl dichloride; water; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; hydrazine; N,N-dimethyl-formamide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;