tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

Base Information

Chemical Name:tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate
CAS No.:1609554-84-8
Molecular Formula:C₁₇H₂₅N₃O₄
Molecular Weight:335.403
Hs Code.:

Synonyms:tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

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Chemical Property of tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

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Technology Process of tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

There total 3 articles about tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 127132-37-0
(S)-Ethyl 3-(4-(allyloxy)phenyl)-2-((tert-butoxycarbonyl)amino) propanoate

: 1609554-84-8
tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

Guidance literature:: With hydrazine; In N,N-dimethyl-formamide; at 80 ℃; for 1h; Inert atmosphere;

Reference yield:

: 127132-38-1
N-(tert-butyloxycarbonyl)-O-allyl-(S)-tyrosine

: 1609554-84-8
tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 80 °C / Inert atmosphere

2: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C / Inert atmosphere

3: hydrazine / N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere

With sulfuric acid; sodium hydrogencarbonate; hydrazine; In tetrahydrofuran; water; N,N-dimethyl-formamide;

Reference yield:

: C₁₄H₁₉NO₃

: 1609554-84-8
tert-butyl (S)-(3-(4-(allyloxy)phenyl)-1-hydrazinyl-1-oxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C / Inert atmosphere

2: hydrazine / N,N-dimethyl-formamide / 1 h / 80 °C / Inert atmosphere

With sodium hydrogencarbonate; hydrazine; In tetrahydrofuran; water; N,N-dimethyl-formamide;