(R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

Base Information

Chemical Name:(R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide
CAS No.:1201698-46-5
Molecular Formula:C₁₈H₁₅ClN₂O₂
Molecular Weight:326.782
Hs Code.:

Synonyms:(R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

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Chemical Property of (R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

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Technology Process of (R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

There total 2 articles about (R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 109-97-7,30604-81-0
pyrrole

: 1201698-31-8
C₁₄H₁₀ClNO₂

: 1201698-46-5
(R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

Guidance literature:: C₁₄H₁₀ClNO₂; With zinc trifluoromethanesulfonate; 2,6-bis<5',5'-diphenyl-4'-(S)-isopropyl oxazolin-2'-yl>pyridine; In chloroform; at -60 - 20 ℃; Inert atmosphere;

pyrrole; In chloroform; at -60 ℃; for 3h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol902360b

Reference yield:

: 109-97-7,30604-81-0
pyrrole

: 883838-74-2
C₁₄H₁₀ClNO₂

: 1201698-46-5
(R)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

: 1383538-69-9
(S)-2-(3-(4-chlorophenyl)-3-(1H-pyrrol-2-yl)propanoyl)pyridine-1-oxide

Guidance literature:: C₁₄H₁₀ClNO₂; With C₃₅H₃₈N₂O₁₂; copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

pyrrole; In dichloromethane; at -30 ℃; for 4h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1039/c2ob25315a