N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

Base Information

Chemical Name:N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine
CAS No.:89708-14-5
Molecular Formula:C₁₆H₁₆Cl₃NO₄
Molecular Weight:392.666
Hs Code.:

Synonyms:N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

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Technology Process of N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

There total 3 articles about N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 79607-51-5,79607-54-8
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-α/β-D-erythro-hex-2-enopyranose

: 545-06-2
trichloroacetonitrile

: 89708-14-5
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

: 89647-31-4
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl amine

Guidance literature:: With sodium hydride; 1.) -40 deg C, 2.) room temperature;
DOI:10.1016/S0040-4039(00)99861-7

Reference yield: 17.0%

: 79607-51-5,79607-54-8
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-α/β-D-erythro-hex-2-enopyranose

: 545-06-2
trichloroacetonitrile

: 89708-14-5
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

: 89647-31-4
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl amine

: 89647-33-6,89708-16-7
N-trichloroacetyl-5-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-D-erythro-hex-2-enofuranosyl amine

: 89647-33-6,89708-16-7
N-trichloroacetyl-5-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enofuranosyl amine

Guidance literature:: With sodium hydride; 1.) -15 deg C, 2.) room temperature;
DOI:10.1016/S0040-4039(00)99861-7

Reference yield:

: 79607-51-5,79607-54-8
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-α/β-D-erythro-hex-2-enopyranose

: 545-06-2
trichloroacetonitrile

: 89708-14-5
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

: 89647-31-4
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-α-D-erythro-hex-2-enopyranosyl amine

: 89708-16-7
5-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-N-trichloracetyl-α-D-erythro-hex-2-enofuranosylamin

: 89647-33-6
5-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-N-trichloracetyl-β-D-erythro-hex-2-enofuranosylamin

Guidance literature:: With sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, RT 2.) -15 deg C; RT, 2 h;
DOI:10.1002/jlac.198619860402