(3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

Base Information

Chemical Name:(3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine
CAS No.:89708-15-6
Molecular Formula:C₁₆H₂₀ClNO₄
Molecular Weight:325.792
Hs Code.:

Synonyms:(3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

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Chemical Property of (3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

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Technology Process of (3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

There total 2 articles about (3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89708-14-5
N-trichloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hex-2-enopyranosyl amine

: 89647-32-5
(3R)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

: 89708-15-6
(3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

Guidance literature:: With hydrogen; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(00)99861-7

Reference yield:

: 79607-51-5,79607-54-8
4-O-Benzoyl-2,3,6-tridesoxy-3-C-methyl-α/β-D-erythro-hex-2-enopyranose

: 89708-15-6
(3S)-N-monochloroacetyl-4-O-benzoyl-2,3,6-trideoxy-3-C-methyl-β-D-erythro-hexopyranosyl amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) CH₂Cl₂, RT 2.) -40 deg C; RT, 2 h

2: H₂ / 10percent Pd/C / methanol / 8 h / 2942.03 Torr

With hydrogen; sodium hydride; palladium on activated charcoal; In methanol;
DOI:10.1002/jlac.198619860402