benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

Base Information

Chemical Name:benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate
CAS No.:1432023-96-5
Molecular Formula:C₂₂H₂₀F₃N₃O₄
Molecular Weight:447.414
Hs Code.:

Synonyms:benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

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Chemical Property of benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

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Technology Process of benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

There total 4 articles about benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1432024-06-0
2-oxo-2-(4-(trifluoromethoxy)phenyl)ethyl 2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetate

: 1432023-96-5
benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

Guidance literature:: With ammonium acetate; In toluene; at 100 - 130 ℃; for 4.5h; Large scale;

Reference yield:

: 1432024-10-6
2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetic acid

: 1432023-96-5
benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / ethyl acetate / Large scale

2: ammonium acetate / toluene / 4.5 h / 100 - 130 °C / Large scale

With ammonium acetate; triethylamine; In ethyl acetate; toluene;

Reference yield:

: 1207175-54-9
3-amino-3-oxetaneacetic acid ethyl ester

: 1432023-96-5
benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / tert-butyl methyl ether / 5 - 20 °C / Large scale

1.2: 18 h / Large scale

2.1: triethylamine / ethyl acetate / Large scale

3.1: ammonium acetate / toluene / 4.5 h / 100 - 130 °C / Large scale

With ammonium acetate; sodium carbonate; triethylamine; In tert-butyl methyl ether; ethyl acetate; toluene;