Ethyl 2-(3-aMinooxetan-3-yl)acetate

Base Information

• Chemical Name: Ethyl 2-(3-aMinooxetan-3-yl)acetate
• CAS No.: 1207175-54-9
• Molecular Formula: C7H13NO3
• Molecular Weight: 159.185
• Hs Code.: 2922390090
• Mol file: 1207175-54-9.mol

Synonyms:Ethyl 2-(3-aMinooxetan-3-yl)acetate;Ethyl 2-(3-aMinooxetan-3-yl)acetate heMioxalate;Ethyl 2-(3-aminooxetan-3-yl)acetate oxalate

Chemical Property of Ethyl 2-(3-aMinooxetan-3-yl)acetate

Chemical Property:

• Boiling Point: 217.4±25.0 °C(Predicted)
• PKA: 7.50±0.20(Predicted)
• PSA: 61.55000
• Density: 1.120±0.06 g/cm3(Predicted)
• LogP: 0.36760
• Storage Temp.: Sealed in dry,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-(3-aminooxetan-3-yl)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 2-(3-aMinooxetan-3-yl)acetate

There total 1 articles about Ethyl 2-(3-aMinooxetan-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl 2-(oxetan-3-ylidene)acetate (922500-91-2) → 3-amino-3-oxetaneacetic acid ethyl ester (1207175-54-9)

Guidance literature:

With ammonia; In ethanol; at 100 ℃; for 5h; Sealed tube;

Reference yield: 73.0%

3-amino-3-oxetaneacetic acid ethyl ester (1207175-54-9) + benzyl chloroformate (501-53-1,94274-21-2) → 2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetic acid (1432024-10-6)

Guidance literature:

3-amino-3-oxetaneacetic acid ethyl ester; benzyl chloroformate; With sodium carbonate; In tert-butyl methyl ether; at 5 - 20 ℃; Large scale;

With water; sodium hydroxide; In tert-butyl methyl ether; for 18h; Large scale;

Reference yield:

3-amino-3-oxetaneacetic acid ethyl ester (1207175-54-9) → 2-oxo-2-(4-(trifluoromethoxy)phenyl)ethyl 2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetate (1432024-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / water / 5 - 20 °C

2: triethylamine / ethyl acetate

With sodium carbonate; triethylamine; In water; ethyl acetate;

DOI:10.1039/c6md00281a

upstream raw materials:

ethyl 2-(oxetan-3-ylidene)acetate

Downstream raw materials:

2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetic acid

3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-amine

benzyl [3-({4-[4-(trifluoromethoxy)phenyl]-1H-imidazol-2-yl}methyl)oxetan-3-yl]carbamate

2-oxo-2-(4-(trifluoromethoxy)phenyl)ethyl 2-(3-(((benzyloxy)carbonyl)amino)oxetan-3-yl)acetate

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