(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

Base Information

Chemical Name:(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane
CAS No.:90032-60-3
Molecular Formula:C₃₄H₃₃NOP₂
Molecular Weight:533.59
Hs Code.:

Synonyms:(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

Chemical Property:

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Technology Process of (1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

There total 1 articles about (1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 299-42-3,7009-81-6,90-83-5,6912-63-6
ephedrine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 90032-60-3
(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

Guidance literature:: With triethylamine; In toluene; at -78 - 20 ℃;
DOI:10.1002/(SICI)1521-3765(20000417)6:8<1496::AID-CHEM1496>3.0.CO;2-8

Reference yield: 63.0%

: 32993-05-8
chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

: 90032-60-3
(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

: chloro(η5-cyclopentadienyl)[(1R,2S)-2-[(diphenylphosphino)methylamino]-1-phenylpropyl diphenylphosphinite-κ2P,P']ruthenium(II)

Guidance literature:: In toluene; mixt. heated in toluene under reflux for 18 h; flash chromy. with CH2Cl2, recrystn. from CH2Cl2/hexane (1/1);
DOI:10.1107/S0108270102018395

Reference yield:

: hydridocarbonyltris(triphenylphosphine)rhodium(I)

: 90032-60-3
(1R,2S)-2-N-Methyl-N-(diphenylphosphino)-2-amino-1-phenyl-1-(diphenylphosphinoxy)propane

: RhH(CO)(L(+)-EPHOS)PPh₃

Guidance literature:: In not given; N2; according to C. Salomon, G. Consiglio, C. Botteghi, P. Pino, Chimia, 27 (1973) 215,;
DOI:10.1016/0022-328X(89)87296-1