2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1583286-84-3
Molecular Formula:C₂₀H₂₅BO₃
Molecular Weight:324.228
Hs Code.:

Synonyms:2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 4 articles about 2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 4'-methoxy-N,N,5-trimethyl-[1,1'-biphenyl]-3-amine

: 73183-34-3
bis(pinacol)diborane

: 1583286-84-3
2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With air; In decane; at 20 ℃; for 48h; Irradiation;
DOI:10.1021/acs.orglett.1c03590

Reference yield:

: 121-72-2
N,N-dimethyl-m-toluidine

: 1583286-84-3
2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1: (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / 24 h / 100 °C / Inert atmosphere

2: palladium diacetate; sodium carbonate / ethanol; water / 16 h / 80 °C / Schlenk technique

3: air / decane / 48 h / 20 °C / Irradiation

With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; palladium diacetate; sodium carbonate; In decane; ethanol; water;
DOI:10.1021/acs.orglett.1c03590

Reference yield:

: N,N-dimethyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborlan-2-yl)-5-methyl benzamine

: 1583286-84-3
2-(4'-methoxy-5-methyl-[1,1'-biphenyl]-3-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; sodium carbonate / ethanol; water / 16 h / 80 °C / Schlenk technique

2: air / decane / 48 h / 20 °C / Irradiation

With palladium diacetate; sodium carbonate; In decane; ethanol; water;
DOI:10.1021/acs.orglett.1c03590