2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

Base Information

Chemical Name:2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine
CAS No.:143573-28-8
Molecular Formula:C₂₇H₂₈N₂O₄
Molecular Weight:444.53
Hs Code.:

Synonyms:2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

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Chemical Property of 2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

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Technology Process of 2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

There total 3 articles about 2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61340-09-8
(2S,4R,5R,6S)-4-<(1R)-1,2-dihydroxyethyl>-5-hydroxy-6-hydroxymethyl-2-phenyl-1,3-dioxane

: 143573-28-8
2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

Guidance literature:: Multi-step reaction with 3 steps

1: NaIO₄ / methanol / 17 h / Ambient temperature

2: HOAc / 4 h / Ambient temperature

3: 1) NaH, 2) tetrabutylammonium chloride / 1) THF, r.t., 1 h, 2) reflux, 2 h

With sodium periodate; tetrabutyl-ammonium chloride; sodium hydride; acetic acid; In methanol;
DOI:10.1016/S0040-4020(01)89027-X

Reference yield:

: 141317-08-0
2,4-O-Benzylidene-L-xylose

: 143573-28-8
2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1: HOAc / 4 h / Ambient temperature

2: 1) NaH, 2) tetrabutylammonium chloride / 1) THF, r.t., 1 h, 2) reflux, 2 h

With tetrabutyl-ammonium chloride; sodium hydride; acetic acid;
DOI:10.1016/S0040-4020(01)89027-X

Reference yield:

: 143573-27-7
2-<(2S,4S,5R,6S)-5-Hydroxy-6-hydroxymethyl-2-phenyl-1,3-dioxan-4-yl>-1,3-diphenylimidazolidine

: 74-95-3
1,1-dibromomethane

: 143573-28-8
2-<(1S,3S,5S,6R)-3-Phenyl-2,4,7,9-tetraoxabicyclo<4.4.0>decan-5-yl>-1,3-diphenylimidazolidine

Guidance literature:: With tetrabutyl-ammonium chloride; sodium hydride; Yield given. Multistep reaction; 1) THF, r.t., 1 h, 2) reflux, 2 h;
DOI:10.1016/S0040-4020(01)89027-X