bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Base Information

Chemical Name:bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane
CAS No.:335164-45-9
Molecular Formula:C₂₃H₄₀OSeSi₂
Molecular Weight:467.701
Hs Code.:

Synonyms:bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Suppliers and Price of bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

There total 3 articles about bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 56310-18-0
di-tert-butylchlorosilane

: 335164-44-8
6-(phenylseleno)-1-trimethylsilyl-1-hexyn-3-ol

: 335164-45-9
bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; for 12h; Heating;
DOI:10.1021/jo001124x

Reference yield:

: 124854-74-6
4-(Phenylseleno)butanal

: 335164-45-9
bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; various solvent(s) / 0.83 h / -78 °C

1.2: 92 percent / tetrahydrofuran; various solvent(s) / 3 h / -78 °C

2.1: 87 percent / imidazole / tetrahydrofuran / 12 h / Heating

With 1H-imidazole; n-butyllithium; In tetrahydrofuran;
DOI:10.1021/jo001124x

Reference yield:

: 1066-54-2
trimethylsilylacetylene

: 335164-45-9
bis(1,1-dimethylethyl)[[1-[3-(phenylseleno)propyl]-3-trimethylsilyl-2-propynyl]oxy]silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; various solvent(s) / 0.83 h / -78 °C

1.2: 92 percent / tetrahydrofuran; various solvent(s) / 3 h / -78 °C

2.1: 87 percent / imidazole / tetrahydrofuran / 12 h / Heating

With 1H-imidazole; n-butyllithium; In tetrahydrofuran;
DOI:10.1021/jo001124x