2-(1-Cyclohexenyl)ethylamine

Base Information

• Chemical Name: 2-(1-Cyclohexenyl)ethylamine
• CAS No.: 3399-73-3
• Molecular Formula: C8H15N
• Molecular Weight: 125.214
• Hs Code.: 29213000
• European Community (EC) Number: 222-267-4
• NSC Number: 26453
• UNII: 88S899CWZ5
• DSSTox Substance ID: DTXSID1063011
• Nikkaji Number: J205.503A
• Wikidata: Q72459783
• Mol file: 3399-73-3.mol

Synonyms:2-(1-cyclohexenyl)ethylamine

Chemical Property of 2-(1-Cyclohexenyl)ethylamine

Chemical Property:

• Appearance/Colour: clear slightly yellow liquid
• Vapor Pressure: 0.378mmHg at 25°C
• Melting Point: -55 °C
• Refractive Index: 1.486-1.488
• Boiling Point: 197.5 °C at 760 mmHg
• PKA: 10.94±0.10(Predicted)
• Flash Point: 57 °C
• PSA: 26.02000
• Density: 0.9 g/cm³
• LogP: 2.53590
• Sensitive.: Air Sensitive
• XLogP3: 1.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 125.120449483
• Heavy Atom Count: 9
• Complexity: 105

Purity/Quality:

99% ^*data from raw suppliers

2-(1-Cyclohexenyl)ethylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): C
• Hazard Codes: C
• Statements: 34
• Safety Statements: 28A-26-45-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(=CC1)CCN
• Uses: 2-(1-Cyclohexenyl)ethylamine has been employed:as substrate for allylic hydroxylation reactionin preparation of thin films and single crystals of 2-(1-cyclohexenyl)ethyl ammonium lead iodide, used to fabricate optoelectronic-compatible heterostructures

Technology Process of 2-(1-Cyclohexenyl)ethylamine

There total 15 articles about 2-(1-Cyclohexenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-cyclohexenylacetonitrile (6975-71-9) → 2-(1-cyclohexenyl)ethylamine (3399-73-3)

Guidance literature:

With sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; at 15 ℃; for 21h; Solvent; Inert atmosphere; Green chemistry;

Reference yield: 88.0%

N-[(3-methyl-2-butenyl)oxycarbonyl]-2-(1-cyclohexenyl)ethylamine (648910-21-8) → 2-(1-cyclohexenyl)ethylamine (3399-73-3)

Guidance literature:

N-[(3-methyl-2-butenyl)oxycarbonyl]-2-(1-cyclohexenyl)ethylamine; With iodine; In methanol; at 20 ℃; for 7h;

With zinc; In methanol; at 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2003.10.058

Reference yield: 80.0%

C14H25N4(1+)*Cl(1-) → 2-(1-cyclohexenyl)ethylamine (3399-73-3)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 80 ℃; for 5h; Temperature; Solvent;

upstream raw materials:

1-cyclohexenylacetonitrile

(cyclohex-1-en-1-yl)-CH₂-CO-NH₂

(2-Cyclohex-1-enyl-ethyl)-carbamic acid benzyl ester

N-[(3-methyl-2-butenyl)oxycarbonyl]-2-(1-cyclohexenyl)ethylamine

Downstream raw materials:

N-(2-cyclohex-1-enylethyl)-2-(4-methoxyphenyl)-acetamide

N-(2-cyclohex-1-enylethyl)formamide

N-(2-cyclohex-1-enyl-ethyl)-malonamic acid ethyl ester

N,N'-bis-(2-cyclohex-1-enyl-ethyl)-malonamide