(S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride

Base Information

• Chemical Name: (S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride
• CAS No.: 1067232-41-0
• Molecular Formula: C₃₀H₂₉NO₂P*Cl
• Molecular Weight: 501.993

Synonyms:(S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride

Chemical Property of (S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride

There total 1 articles about (S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(S)-N(3)-chloromethyl-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-39-6) + triphenylphosphine (603-35-0) → (S)-N(3)-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride (1067232-41-0)

Guidance literature:

In acetonitrile; at 20 ℃; for 24h;

DOI:10.1016/j.tet.2008.07.012

Reference yield: 76.0%

(S)-N(3)-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride (1067232-41-0) + benzaldehyde (100-52-7) → (S)-N(3)-methyl-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-46-5) + (S,Z)-N(3)-(2'-phenylethenyl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-44-3) + (4S,1'E)-3-(2'-phenylethenyl)-5,5-dimethyl-4-phenyloxazolidin-2-one (636580-91-1)

Guidance literature:

(S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 0.5h;

benzaldehyde; In tetrahydrofuran; at -78 ℃; for 24h; Further stages.;

DOI:10.1016/j.tet.2008.07.012

Reference yield: 63.0%

(S)-N(3)-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride (1067232-41-0) + acetaldehyde (75-07-0,9002-91-9) → (S,Z)-N(3)-(prop-1'-en-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one (1067232-48-7)

Guidance literature:

(S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 0.5h;

acetaldehyde; In tetrahydrofuran; at -78 ℃; for 24h; Further stages.;

DOI:10.1016/j.tet.2008.07.012

upstream raw materials:

(S)-N⁽³⁾-chloromethyl-4-phenyl-5,5-dimethyloxazolidin-2-one

triphenylphosphine

Downstream raw materials:

(S)-N⁽³⁾-methyl-4-phenyl-5,5-dimethyloxazolidin-2-one

(S,Z)-N⁽³⁾-(2'-phenylethenyl)-4-phenyl-5,5-dimethyloxazolidin-2-one

(4S,1'E)-3-(2'-phenylethenyl)-5,5-dimethyl-4-phenyloxazolidin-2-one

(S,Z)-N⁽³⁾-(prop-1'-en-1'-yl)-4-phenyl-5,5-dimethyloxazolidin-2-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1067232-41-0 (S)-N⁽³⁾-[(triphenylphosphonium)methyl]-4-phenyl-5,5-dimethyloxazolidin-2-one chloride

Send

Send

Metric Ton KG G Pound L ML

Send

Send