N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

Base Information

Chemical Name:N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine
CAS No.:1071529-01-5
Molecular Formula:C₂₈H₂₀N₆O₂
Molecular Weight:472.506
Hs Code.:

Synonyms:N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

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Chemical Property of N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

Chemical Property:

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Technology Process of N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

There total 3 articles about N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8-(6-bromopyridin-3-yloxy)-3-methoxy-1,5-naphthyridine

: 18584-59-3
3-amino-8-phenylbenzopyridazine

: 1071529-01-5
N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tert-butyl XPhos; In toluene; at 100 ℃; for 24h; Inert atmosphere; Sealed tube;

Reference yield:

: 10132-01-1
1-chloro-4-phenyl-phthalazine

: 1071529-01-5
N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / tert-butyl alcohol / 17 h / 100 °C / Inert atmosphere; Sealed tube

2: hydrogen bromide / water; acetic acid / 3 h / 90 °C / Sealed tube

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tert-butyl XPhos / toluene / 24 h / 100 °C / Inert atmosphere; Sealed tube

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; hydrogen bromide; caesium carbonate; sodium t-butanolate; tert-butyl XPhos; In water; acetic acid; toluene; tert-butyl alcohol;

Reference yield:

: N-(2,4-dimethoxybenzyl)-4-phenylphthalazin-1-amine

: 1071529-01-5
N-(5-(7-methoxy-1,5-naphthyridin-4-yloxy)pyridin-2-yl)-4-phenylphthalazin-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide / water; acetic acid / 3 h / 90 °C / Sealed tube

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; tert-butyl XPhos / toluene / 24 h / 100 °C / Inert atmosphere; Sealed tube

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; hydrogen bromide; sodium t-butanolate; tert-butyl XPhos; In water; acetic acid; toluene;