(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

Base Information

Chemical Name:(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine
CAS No.:152984-31-1
Molecular Formula:C₂₇H₃₃NO₄SSi
Molecular Weight:495.715
Hs Code.:

Synonyms:(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

Chemical Property:

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Technology Process of (2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

There total 3 articles about (2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Acetic acid (2R,3S)-3-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-aziridin-2-ylmethyl ester

: 152984-31-1
(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

Guidance literature:: With potassium carbonate; In methanol; at 0 ℃; for 0.25h; Yield given;
DOI:10.3987/COM-95-S76

Reference yield:

: 132835-12-2
Acetic acid (2R,3S)-3-hydroxymethyl-1-(toluene-4-sulfonyl)-aziridin-2-ylmethyl ester

: 152984-31-1
(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 0.5 h / 0 °C

2: potassium carbonate / methanol / 0.25 h / 0 °C

With 1H-imidazole; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-95-S76

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 152984-31-1
(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 0.5 h / 0 °C

2: potassium carbonate / methanol / 0.25 h / 0 °C

With 1H-imidazole; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-95-S76