(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

Base Information

Chemical Name:(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine
CAS No.:174096-42-5
Molecular Formula:C₃₅H₄₀N₂O₅SSi
Molecular Weight:628.865
Hs Code.:

Synonyms:(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

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Technology Process of (2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

There total 4 articles about (2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3173-56-6
benzyl isothiocyanate

: 152984-31-1
(2S,3R)-2-tert-butyldiphenylsilyloxymethyl-3-hydroxymethyl-N-tosylaziridine

: 174096-42-5
(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In toluene; 50 deg C, 4 h, 80 deg C, 4 h;
DOI:10.3987/COM-95-S76

Reference yield:

: 132835-12-2
Acetic acid (2R,3S)-3-hydroxymethyl-1-(toluene-4-sulfonyl)-aziridin-2-ylmethyl ester

: 174096-42-5
(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 0.5 h / 0 °C

2: potassium carbonate / methanol / 0.25 h / 0 °C

3: 85 percent / N,N-diisopropylethylamine / toluene / 50 deg C, 4 h, 80 deg C, 4 h

With 1H-imidazole; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-95-S76

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 174096-42-5
(2S,3R)-3-benzylcarbamoyloxymethyl-2-tert-butyldiphenylsilyloxymethyl-N-tosylaziridine

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 0.5 h / 0 °C

2: potassium carbonate / methanol / 0.25 h / 0 °C

3: 85 percent / N,N-diisopropylethylamine / toluene / 50 deg C, 4 h, 80 deg C, 4 h

With 1H-imidazole; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-95-S76