2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

Base Information

Chemical Name:2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate
CAS No.:1032678-13-9
Molecular Formula:C₃₆H₄₈N₃O₂*F₆P
Molecular Weight:699.76
Hs Code.:

2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

Synonyms:2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

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Chemical Property of 2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

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Technology Process of 2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

There total 1 articles about 2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1032678-01-5
2-[3-(1,3,3-trimethyl-2,3-dihydro-1H-indol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolium chloride

: 50910-54-8
trans-4-aminocyclohexanol hydrochloride

: 1032678-13-9
2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

Guidance literature:: 2-[3-(1,3,3-trimethyl-2,3-dihydro-1H-indol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-(5-carboxypentyl)-3H-indolium chloride; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

trans-4-aminocyclohexanol hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1002/ejoc.200701190

Reference yield: 93.0%

: 1032678-13-9
2-[3-(1,3,3-trimethyl-2,3-dihydroindol-2-ylidene)-1-propenyl]-3,3-dimethyl-1-[5-(trans-4-hydroxycyclohexylaminocarbonyl)pentyl]-3H-indolium hexafluorophosphate

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 2-[3-(1,3,3-trimethyl-2,3-dihydro-1H-indol-2-ylidene)-1-propenyl]-1-{5-[trans-4-(diisopropylamino-2-cyanoethoxyphosphanyloxy)-cyclohexylaminocarbonyl]pentyl}-3,3-dimethyl-3H-indolium hexafluorophosphate

Guidance literature:: With N,N-diisopropylamine tetrazolide; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.200701190