C₄₂H₄₅NO₆

Base Information

• Chemical Name: C₄₂H₄₅NO₆
• CAS No.: 1233956-73-4
• Molecular Formula: C₄₂H₄₅NO₆
• Molecular Weight: 659.822
• Mol file: 1233956-73-4.mol

Synonyms:C₄₂H₄₅NO₆

Chemical Property of C₄₂H₄₅NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₄₅NO₆

There total 2 articles about C₄₂H₄₅NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-D-1-O-(4-methoxybenzyl)-3,4,5,6-tetra-O-benzyl-scyllo-inosose → C42H45NO6 (1233956-73-4)

Guidance literature:

With ammonium acetate; sodium cyanoborohydride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1039/b9nj00629j

Reference yield:

3,4,5,6-tetra-O-benzyl-1-O-p-methoxybenzyl-D-myo-inositol (170900-81-9) → C42H45NO6 (1233956-73-4)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic anhydride; dimethyl sulfoxide / 14 h / 20 °C / Inert atmosphere

2: ammonium acetate; sodium cyanoborohydride / tetrahydrofuran / 2 h / 20 °C

With ammonium acetate; acetic anhydride; sodium cyanoborohydride; dimethyl sulfoxide; In tetrahydrofuran; 1: Swern oxidation;

DOI:10.1039/b9nj00629j

Reference yield: 90.0%

C42H45NO6 (1233956-73-4) + benzyl chloroformate (501-53-1,94274-21-2) → 1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol (1233956-74-5)

Guidance literature:

With potassium carbonate; In 1,4-dioxane; water; for 1h; Inert atmosphere;

DOI:10.1039/b9nj00629j

upstream raw materials:

3,4,5,6-tetra-O-benzyl-1-O-p-methoxybenzyl-D-myo-inositol

Downstream raw materials:

1-D-2-deoxy-2-N-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol

1-D-1-O-(4-methoxybenzyl)-2-deoxy-2-benzyloxycarbonylamino-3,4,5,6-tetra-O-benzyl-myo-inositol