dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester

Base Information

• Chemical Name: dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester
• CAS No.: 854278-30-1
• Molecular Formula: C₁₃H₁₇ClN₂O₂Se₂
• Molecular Weight: 426.663

Synonyms:dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester

Chemical Property of dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester

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Technology Process of dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester

There total 1 articles about dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

bis(N,N-dimethylcarbamoyl) diselenide (36598-11-5) + 1-chloro-3-(dibromomethyl)benzene (70288-97-0) → dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester (854278-30-1)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 9h;

DOI:10.1002/hc.20190

Reference yield: 91.0%

dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester (854278-30-1) → 2,4,6-tris-(3-chloro-phenyl)-[1,3,5]triselenane

Guidance literature:

With tin(IV) chloride; In benzene; at 20 ℃; for 6h;

DOI:10.1002/hc.20190

Reference yield: 33.0%

dimethyl-selenocarbamic acid Se-[(3-chloro-phenyl)-dimethylcarbamoylselanyl-methyl] ester (854278-30-1) + 2,3-dimethyl-buta-1,3-diene (513-81-5) → 2-(3-chloro-phenyl)-4,5-dimethyl-3,6-dihydro-2H-selenopyran

Guidance literature:

With tin(IV) chloride; In benzene; at 20 ℃;

DOI:10.1002/hc.20190

upstream raw materials:

bis(N,N-dimethylcarbamoyl) diselenide

1-chloro-3-(dibromomethyl)benzene

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