Technology Process of C16H22O6
There total 4 articles about C16H22O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 26 °C
1.2: 0.5 h / 0 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 26 °C
3.1: pyridine / tetrahydrofuran / 5 h / 26 °C
4.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C
5.1: potassium hydroxide; water / methanol / 0 °C
With
pyridine; 1H-imidazole; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; water; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C
2: potassium hydroxide; water / methanol / 0 °C
With
trimethylsilyl trifluoromethanesulfonate; water; potassium hydroxide;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 26 °C
2: pyridine / tetrahydrofuran / 5 h / 26 °C
3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0 °C
4: potassium hydroxide; water / methanol / 0 °C
With
pyridine; trimethylsilyl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; water; potassium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;