(4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

Base Information

Chemical Name:(4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine
CAS No.:99948-63-7
Molecular Formula:C₁₆H₂₃ClN₂O₂
Molecular Weight:310.824
Hs Code.:

Synonyms:(4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

Suppliers and Price of (4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

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Technology Process of (4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

There total 2 articles about (4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 917-95-3
t-butylnitrite

: 1885-81-0
p-chlorophenyl isocyanide

: 630-19-3
pivalaldehyde

: 99948-63-7
(4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

Guidance literature:: In benzene; at 100 ℃; for 24h;
DOI:10.1021/jo00355a028

Reference yield:

: 99948-61-5
[2,5-Di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-phenyl-amine

: 99948-63-7
(4-Chloro-phenyl)-[2,5-di-tert-butyl-[1,4,2]dioxazolidin-(3Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / tetrahydrofuran / 2 h / Ambient temperature

2: 56 percent / benzene / 24 h / 100 °C

With sulfuric acid; In tetrahydrofuran; benzene;
DOI:10.1021/jo00355a028