Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

(2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine

Base Information Edit
  • Chemical Name:(2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine
  • CAS No.:90762-27-9
  • Molecular Formula:C33H37NO6
  • Molecular Weight:543.66
  • Hs Code.:
  • Mol file:90762-27-9.mol
(2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine

Synonyms:(2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine

Suppliers and Price of (2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of (2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine Edit
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of (2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine

There total 27 articles about (2R,3S,4R)-1-acetyl-3,4-dibenzyloxy-2-<(1R,2Z)-1-benzyloxy-3-ethoxycarbonyl-2-propenyl>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 9 steps
1: 1.) 2M HCl; 2.) pyridine / 1.) reflux, 13 h; 2.) overnight
2: 1.) sodium methoxide / 1.) MeOH, 2 h; 2.) conc. HCl, -15 deg C, 7 h
3: 4-dimethylaminopyridine / pyridine / 3.5 h / 70 °C
4: 1.) sodium hydride / 1.) DMF, 20 min; 2.) DMF, overnight
5: toluene-p-sulfonic acid monohydrate / methanol / 2 h
6: 77 percent / pyridine / 16 h
7: 93 percent / aq. sodium hydroxide / dioxane / 0.5 h / Heating
8: mercury(II) chloride, calcium carbonate / H2O; acetonitrile / 0.83 h
9: 2 percent / 60percent sodium hydride in mineral oil / tetrahydrofuran / 4 h
With pyridine; hydrogenchloride; dmap; sodium hydroxide; sodium methylate; sodium hydride; toluene-4-sulfonic acid; calcium carbonate; mercury dichloride; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; water; acetonitrile;
DOI:10.1016/0008-6215(85)85186-7
Guidance literature:
Multi-step reaction with 11 steps
1: 97 percent / 0.5percent aq. HCl / methanol / 1 h / Heating
2: 1.) sodium acetate; 2.) pyridine / 1.) water, 2-methoxyethanol, 25 h, reflux; 2.) 3 h
3: 1.) 2M HCl; 2.) pyridine / 1.) reflux, 13 h; 2.) overnight
4: 1.) sodium methoxide / 1.) MeOH, 2 h; 2.) conc. HCl, -15 deg C, 7 h
5: 4-dimethylaminopyridine / pyridine / 3.5 h / 70 °C
6: 1.) sodium hydride / 1.) DMF, 20 min; 2.) DMF, overnight
7: toluene-p-sulfonic acid monohydrate / methanol / 2 h
8: 77 percent / pyridine / 16 h
9: 93 percent / aq. sodium hydroxide / dioxane / 0.5 h / Heating
10: mercury(II) chloride, calcium carbonate / H2O; acetonitrile / 0.83 h
11: 2 percent / 60percent sodium hydride in mineral oil / tetrahydrofuran / 4 h
With pyridine; hydrogenchloride; dmap; sodium hydroxide; sodium methylate; sodium acetate; sodium hydride; toluene-4-sulfonic acid; calcium carbonate; mercury dichloride; In tetrahydrofuran; 1,4-dioxane; pyridine; methanol; water; acetonitrile;
DOI:10.1016/0008-6215(85)85186-7
Post RFQ for Price