C₃₉H₅₄N₂O₆SSi

Base Information

Chemical Name:C₃₉H₅₄N₂O₆SSi
CAS No.:910558-58-6
Molecular Formula:C₃₉H₅₄N₂O₆SSi
Molecular Weight:707.019
Hs Code.:

C<sub>39</sub>H<sub>54</sub>N<sub>2</sub>O<sub>6</sub>SSi

Synonyms:C₃₉H₅₄N₂O₆SSi

Suppliers and Price of C₃₉H₅₄N₂O₆SSi

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₉H₅₄N₂O₆SSi

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₉H₅₄N₂O₆SSi

There total 12 articles about C₃₉H₅₄N₂O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 910558-57-5
C₃₉H₅₄N₂O₇Si

: 910558-58-6
C₃₉H₅₄N₂O₆SSi

: C₃₉H₅₄N₂O₆SSi

Guidance literature:: With Lawessons reagent; In toluene; at 110 ℃; for 3h;
DOI:10.1021/ol051975x

Reference yield:

: 202807-44-1
6-methoxy-1-methyl-1H-indole-3-carbaldehyde

: 910558-58-6
C₃₉H₅₄N₂O₆SSi

Guidance literature:: Multi-step reaction with 10 steps

1.1: 99 percent / NH₄OAc / 1 h / Heating

2.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3.1: ethanol / 25 °C

3.2: 64 percent / N₂H₄*H₂O / ethanol / 5 h / Heating

4.1: 61 percent / EDCI; DMAP / CH₂Cl₂ / 19 h / 25 °C

5.1: 67 percent / p-toluenesulfonyl chloride; Et₃N / CH₂Cl₂ / 20 h / 25 °C

6.1: 96 percent / EDCI; DMAP / CH₂Cl₂ / 16 h / 0 - 25 °C

7.1: 53 percent / various solvent(s) / 90 h / 230 °C

8.1: Chiracel OD / propan-2-ol; hexane

9.1: LDA; bis(trimethylsilyl)peroxide / tetrahydrofuran / 4 h / -40 °C

9.2: 64 percent / tetrahydrofuran / 2 h / -40 - 20 °C

10.1: 70 percent / Lawesson's reagent / toluene / 3 h / 110 °C

With Lawessons reagent; dmap; lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; Chiracel OD; ammonium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; p-toluenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; isopropyl alcohol; toluene;
DOI:10.1021/ol051975x

Reference yield:

: 6-methoxy-1-methyl-3-(2-nitrovinyl)-1H-indole

: 910558-58-6
C₃₉H₅₄N₂O₆SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2.1: ethanol / 25 °C

2.2: 64 percent / N₂H₄*H₂O / ethanol / 5 h / Heating

3.1: 61 percent / EDCI; DMAP / CH₂Cl₂ / 19 h / 25 °C

4.1: 67 percent / p-toluenesulfonyl chloride; Et₃N / CH₂Cl₂ / 20 h / 25 °C

5.1: 96 percent / EDCI; DMAP / CH₂Cl₂ / 16 h / 0 - 25 °C

6.1: 53 percent / various solvent(s) / 90 h / 230 °C

7.1: Chiracel OD / propan-2-ol; hexane

8.1: LDA; bis(trimethylsilyl)peroxide / tetrahydrofuran / 4 h / -40 °C

8.2: 64 percent / tetrahydrofuran / 2 h / -40 - 20 °C

9.1: 70 percent / Lawesson's reagent / toluene / 3 h / 110 °C

With Lawessons reagent; dmap; lithium aluminium tetrahydride; bis-trimethylsilanyl peroxide; Chiracel OD; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; p-toluenesulfonyl chloride; lithium diisopropyl amide; In tetrahydrofuran; ethanol; hexane; dichloromethane; isopropyl alcohol; toluene;
DOI:10.1021/ol051975x