C₂₃H₃₀O₅Se

Base Information

Chemical Name:C₂₃H₃₀O₅Se
CAS No.:75948-66-2
Molecular Formula:C₂₃H₃₀O₅Se
Molecular Weight:465.448
Hs Code.:

C<sub>23</sub>H<sub>30</sub>O<sub>5</sub>Se

Synonyms:C₂₃H₃₀O₅Se

Suppliers and Price of C₂₃H₃₀O₅Se

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of C₂₃H₃₀O₅Se

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of C₂₃H₃₀O₅Se

There total 35 articles about C₂₃H₃₀O₅Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₃H₂₈O₅Se

: 75948-66-2
C₂₃H₃₀O₅Se

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 12h;
DOI:10.1021/ja00543a063

Reference yield:

: C₂₃H₂₈O₅Se

: 75948-66-2
C₂₃H₃₀O₅Se

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 12h;
DOI:10.1021/ja00543a063

Reference yield:

: 61934-55-2
3-bromomethyl-2-butenolide

: 75948-66-2
C₂₃H₃₀O₅Se

Guidance literature:: Multi-step reaction with 8 steps

1: 90 percent / Heating

2: 80 percent / NaH / dimethylformamide / 0.5 h / -5 - 0 °C

3: 2.) KO-t-Bu / 1.) toluene, 200 deg C, 0.5 h, 2.) ether, 0 deg C, 0.5 h

4: p-TsOH / methanol / 12 h / 65 °C

5: NEt₃ / CH₂Cl₂ / 0.5 h / -5 °C

6: DBU / tetrahydrofuran / 8 h / 65 °C

7: 92 percent / 2 h / Ambient temperature

8: 95 percent / DIBAL-H / toluene; tetrahydrofuran / 12 h / -78 °C

With potassium tert-butylate; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja00543a063