10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene

Base Information

• Chemical Name: 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene
• CAS No.: 157056-97-8
• Molecular Formula: C₂₆H₃₈O₇
• Molecular Weight: 462.584

Synonyms:10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene

Chemical Property of 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene

Chemical Property:

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Technology Process of 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene

There total 8 articles about 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

taxuyunnanin C (156127-34-3) → 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene (157056-97-8) + (3S,4aS,5S,6S,7S,11S,12aS)-1,2,3,4,4a,5,6,7,8,11,12,12a-dodecahydro-9,12a,13,13-tetramethyl-4-methylene-6,10-methanobenzocyclodecene-3,5,7,11-tetrol 5-acetate (849705-68-6) + 10β,14β-dihydroxy-2α,5α-diacetoxy-4(20),11-taxadiene (167355-42-2)

Guidance literature:

With sodium hydroxide; In methanol; at 30 ℃;

DOI:10.1016/S0031-9422(98)00674-8

Reference yield: 40.0%

taxuyunnanin C (156127-34-3) → 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene (157056-97-8) + 14β-hydroxy-2α,5α,10β-triacetoxy-4(20),11-taxadiene (191536-23-9)

Guidance literature:

With potassium hydroxide; In tetrahydrofuran; methanol; at 0 ℃; for 0.333333h;

DOI:10.1016/j.bmcl.2004.06.089

Reference yield: 36.3%

taxuyunnanin C (156127-34-3) → 10β-hydroxy-2α,5α14β-triacetoxytaxa-4(20),11(12)-diene (157056-97-8)

Guidance literature:

With potassium hydroxide; In methanol; at 0 ℃; for 0.5h;

DOI:10.1021/ol301755n

upstream raw materials:

taxuyunnanin C

Downstream raw materials:

taxuyunnanin C

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