t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Base Information

Chemical Name:t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane
CAS No.:1245635-33-9
Molecular Formula:C₁₈H₃₀BIO₃Si
Molecular Weight:460.235
Hs Code.:

Synonyms:t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Suppliers and Price of t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

There total 4 articles about t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 1245635-32-8
{3-[(t-butyldimethylsilyl)oxy]-2-iodophenyl}boronic acid

: 1245635-33-9
t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Guidance literature:: In dichloromethane; Inert atmosphere;
DOI:10.1002/anie.201002191

Reference yield:

: 1245635-31-7
t-butyl(2,3-diiodophenoxy)dimethylsilane

: 1245635-33-9
t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: dichloromethane

With isopropylmagnesium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.03.016

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1245635-33-9
t-butyl[2-iodo-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenoxy]dimethylsilane

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: dichloromethane

With 1H-imidazole; isopropylmagnesium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tet.2013.03.016