Q₈₂₄₁

Base Information

• Chemical Name: Q₈₂₄₁
• CAS No.: 153181-59-0
• Molecular Formula: C₄₈H₄₆N₄O₄
• Molecular Weight: 742.918

Synonyms:Q₈₂₄₁

Chemical Property of Q₈₂₄₁

Chemical Property:

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Technology Process of Q₈₂₄₁

There total 5 articles about Q₈₂₄₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2R,3S,4S,5R)-2,5-bis[N-(benzyloxycarbonyl)amino]-1,6-diphenyl-3,4-hexanediol (153223-10-0) → Q8241 (153181-59-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 100 percent / diisopropylethylamine / dimethylformamide / 16 h / Ambient temperature

2: 99 percent / H₂ / 5percent Pd/C / ethanol / 1.5 h

3: 60.9 percent / pyridine / 2 h / 125 °C

4: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 18 h

5: HCl / dioxane / Ambient temperature

With pyridine; hydrogenchloride; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm970524i

Reference yield:

dibenzyl ((2R,3S,4S,5R)-1,6-diphenyl-3,4-bis((2-(trimethylsilyl)ethoxy)methoxy)hexane-2,5-diyl)dicarbamate (153181-18-1) → Q8241 (153181-59-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 99 percent / H₂ / 5percent Pd/C / ethanol / 1.5 h

2: 60.9 percent / pyridine / 2 h / 125 °C

3: 1.) NaH / 1.) DMF, RT, 30 min, 2.) DMF, RT, 18 h

4: HCl / dioxane / Ambient temperature

With pyridine; hydrogenchloride; hydrogen; sodium hydride; palladium on activated charcoal; In 1,4-dioxane; ethanol;

DOI:10.1021/jm970524i

Reference yield:

(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-(4-benzyloxy-benzyl)-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide (153181-58-9) → Q8241 (153181-59-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; Yield given; Ambient temperature;

DOI:10.1021/jm970524i

upstream raw materials:

(4R,5S,6S,7R)-4,7-Dibenzyl-1,3-bis-(4-benzyloxy-benzyl)-5,6-bis-(2-trimethylsilanyl-ethoxymethoxy)-[1,3]diazepan-2-ylidene-cyanamide

(2R,3S,4S,5R)-2,5-bis[N-(benzyloxycarbonyl)amino]-1,6-diphenyl-3,4-hexanediol

(2R,3S,4S,5R)-1,6-diphenyl-3,4-bis((2-(trimethylsilyl)ethoxy)methoxy)hexane-2,5-diamine

dibenzyl ((2R,3S,4S,5R)-1,6-diphenyl-3,4-bis((2-(trimethylsilyl)ethoxy)methoxy)hexane-2,5-diyl)dicarbamate

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