exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane

Base Information

Chemical Name:exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane
CAS No.:497163-57-2
Molecular Formula:C₂₄H₃₀N₂O₂
Molecular Weight:378.514
Hs Code.:
Mol file:497163-57-2.mol

Synonyms:tert-butyl (1R,5S,6s)-6-(N,N-dibenzylamino)-3-azabicyclo[3.1.0]hexane-3-carboxylate

Suppliers and Price of exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane

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Technology Process of exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane

There total 1 articles about exo-1-Boc-6-[bis(phenylMethyl)aMino]-3-aza-bicyclo[3.1.0]hexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5464-77-7
N,N-dibenzylformamide

: 73286-70-1
N-(tert-butoxycarbonyl)-3-pyrroline

: 497163-57-2
tert-butyl (1R,5S,6s)-6-(N,N-dibenzylamino)-3-azabicyclo[3.1.0]hexane-3-carboxylate

Guidance literature:: With titanium(IV) isopropylate; methylmagnesium chloride; cyclohexylmagnesium bromide; In tetrahydrofuran; diethyl ether; for 0.25h; Heating;
DOI:10.1002/1521-3765(20020816)8:16<3789::AID-CHEM3789>3.0.CO;2-R

Reference yield: 99.0%

: 497163-57-2
tert-butyl (1R,5S,6s)-6-(N,N-dibenzylamino)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 210482-10-3
1α,5α,6α-6-dibenzylamino-3-azabicyclo[3.1.0]hexane

Guidance literature:: tert-butyl (1R,5S,6s)-6-(N,N-dibenzylamino)-3-azabicyclo[3.1.0]hexane-3-carboxylate; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

With water; sodium hydrogencarbonate; In chloroform;

Reference yield: 98.0%

: 497163-57-2
tert-butyl (1R,5S,6s)-6-(N,N-dibenzylamino)-3-azabicyclo[3.1.0]hexane-3-carboxylate

: 2256715-14-5,273206-92-1,1453252-65-7
tert-butyl (1S,3R,5R)-6-amino-3-azabicyclo[3.1.0]hexane-3-carboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h;
DOI:10.1002/1521-3765(20020816)8:16<3789::AID-CHEM3789>3.0.CO;2-R