(2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate

Base Information

Chemical Name:(2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate
CAS No.:1126386-89-7
Molecular Formula:C₃₂H₄₀O₉Si
Molecular Weight:596.75
Hs Code.:

Synonyms:(2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate

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Technology Process of (2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate

There total 1 articles about (2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1126386-90-0
C₁₁H₁₆O₇

: 108-24-7
acetic anhydride

: 88159-06-2
tert-butyl(diphenyl)(2-propynyloxy)silane

: 1126386-89-7
(2S,3S,4S,5S)-8-(tert-butyldiphenylsilyloxy)oct-6-yne-2,3,4,5-tetrayl tetraacetate

Guidance literature:: tert-butyl(diphenyl)(2-propynyloxy)silane; With (1S,2R)-(+)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine; In toluene; for 0.5h; Inert atmosphere;

C₁₁H₁₆O₇; In toluene; for 2.5h; Inert atmosphere;

acetic anhydride; With dmap; triethylamine; In dichloromethane; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo8025753