2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

Base Information

Chemical Name:2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine
CAS No.:123956-67-2
Molecular Formula:C₃₅H₃₅NO₁₂
Molecular Weight:661.662
Hs Code.:

Synonyms:2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

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Chemical Property of 2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

Chemical Property:

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Technology Process of 2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

There total 1 articles about 2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 98-88-4
benzoyl chloride

: 22435-65-0
N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 123956-66-1
2,3,4,6-tetra-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 123956-67-2
2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 123956-68-3
3,6-di-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

Guidance literature:: In pyridine; at 0 ℃; for 24h;
DOI:10.1016/0008-6215(89)84056-X

Reference yield: 78.0%

: 123956-67-2
2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 123956-73-0
2,3,6-tri-O-benzoyl-β-D-galactopyranosylamine hydrobromide

Guidance literature:: With bromine; In chloroform; water; for 48h; Ambient temperature;
DOI:10.1016/0008-6215(89)84056-X

Reference yield:

: 123956-67-2
2,3,6-tri-O-benzoyl-N-(2,2-diethoxycarbonylvinyl)-β-D-galactopyranosylamine

: 123956-75-2
2,3,6-tri-O-benzoyl-β-D-galactopyranosyl isothiocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / bromine / CHCl₃; H₂O / 48 h / Ambient temperature

2: 54 percent / CaCO₃ / CHCl₃; H₂O / 48 h

With bromine; calcium carbonate; In chloroform; water;
DOI:10.1016/0008-6215(89)84056-X