(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

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Chemical Name:(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one
CAS No.:1383720-86-2
Molecular Formula:C₁₉H₁₇N₅O₅
Molecular Weight:395.374
Hs Code.:

Synonyms:(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

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Technology Process of (3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

There total 4 articles about (3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 66544-68-1
L-(-)-proline hydrazide

: 555-16-8
4-nitrobenzaldehdye

: 1383720-86-2
(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

Guidance literature:: In ethanol; at 20 ℃;
DOI:10.1016/j.tetasy.2012.05.010

Reference yield:

: 955-40-8,172478-10-3
N-benzyl-L-proline ethyl ester

: 1383720-86-2
(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / methanol / 16 h / 20 °C

2: palladium 10% on activated carbon; ammonium formate / methanol / 1 h / Reflux

3: ethanol / 20 °C

With palladium 10% on activated carbon; ammonium formate; hydrazine hydrate; In methanol; ethanol;
DOI:10.1016/j.tetasy.2012.05.010

Reference yield:

: 911429-36-2
(2S)-1-benzylpyrrolidine-2-carbohydrazide

: 1383720-86-2
(3R,7aS)-3-(4-nitrophenyl)-2-{[(E)-(4-nitrophenyl)methyliden]amino}hexahydro-1H-pyrrolo[1,2-c]imidazol-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; ammonium formate / methanol / 1 h / Reflux

2: ethanol / 20 °C

With palladium 10% on activated carbon; ammonium formate; In methanol; ethanol;
DOI:10.1016/j.tetasy.2012.05.010