Technology Process of 6-methoxy-3-nitrobenzylthioacetic acid
There total 3 articles about 6-methoxy-3-nitrobenzylthioacetic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jm200570p
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol / 1 h / 0 - 5 °C / Inert atmosphere
2: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere
3: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; phosphorus tribromide; sodium hydroxide;
In
methanol; toluene;
DOI:10.1021/jm200570p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: phosphorus tribromide / toluene / 0.5 h / 40 - 100 °C / Inert atmosphere
2: sodium hydroxide / methanol / 3 h / 20 °C / Inert atmosphere
With
phosphorus tribromide; sodium hydroxide;
In
methanol; toluene;
DOI:10.1021/jm200570p
