1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

Base Information

Chemical Name:1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene
CAS No.:952658-49-0
Molecular Formula:C₄₀H₆₀N₆O₁₀S₂
Molecular Weight:849.083
Hs Code.:

Synonyms:1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

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Chemical Property of 1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

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Technology Process of 1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

There total 1 articles about 1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 952658-45-6
1,2-bis(2-{4'-[4'-(methylphenyl)sulphonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-dinitrobenzene

: 952658-49-0
1,2-bis(2-{4'-[4'-(methylphenyl)sulfonyl]-1',7'-dioxa-4',10'-diazacyclododecane}ethoxy)-4,5-diaminobenzene

Guidance literature:: With 10% palladium on charcoal; hydrazine hydrate; In butan-1-ol; for 10.5h; Reflux; Inert atmosphere;
DOI:10.1246/bcsj.80.1549