2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

Base Information

Chemical Name:2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol
CAS No.:528609-01-0
Molecular Formula:C₄₃H₄₃O₂P₃
Molecular Weight:684.734
Hs Code.:

Synonyms:2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

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Chemical Property of 2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

Chemical Property:

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Technology Process of 2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

There total 7 articles about 2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 829-85-6
diphenylphosphane

: 528608-99-3
2-(3-chloro-2,2-bis-chloromethyl-propoxy)-ethanol

: 528609-01-0
2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

Guidance literature:: With potassium hydroxide; potassium carbonate; In dimethyl sulfoxide; at 90 - 110 ℃;
DOI:10.1002/ejic.200390019

Reference yield:

: 19309-39-8
1-methyl-4-(hydroxymethyl)-2,6,7-trioxabicyclo-[2.2.2]-octane

: 528609-01-0
2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / KOH / dimethylsulfoxide / 2 h / 60 °C

2: 86 percent / aq. HCl / methanol / 6 h / 20 °C

3: 56 percent / SOCl₂; pyridine / 0 - 120 °C

4: 81 percent / hydrogen / Pd/C / tetrahydrofuran / 12 h / 20 °C / 750.06 Torr

5: 73 percent / aq. KOH; K₂CO₃ / dimethylsulfoxide / 90 - 110 °C

With pyridine; hydrogenchloride; potassium hydroxide; thionyl chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1002/ejic.200390019

Reference yield:

: 528608-98-2
[2-(3-chloro-2,2-bis-chloromethyl-propoxy)-ethoxymethyl]-benzene

: 528609-01-0
2-{3-diphenylphosphanyl-2,2-bis-[(diphenylphosphanyl)-methyl]-propoxy}-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / hydrogen / Pd/C / tetrahydrofuran / 12 h / 20 °C / 750.06 Torr

2: 73 percent / aq. KOH; K₂CO₃ / dimethylsulfoxide / 90 - 110 °C

With potassium hydroxide; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1002/ejic.200390019