N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

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Chemical Name:N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide
CAS No.:1606142-75-9
Molecular Formula:C₂₈H₂₄N₆O₁₂S₂
Molecular Weight:700.664
Hs Code.:

Synonyms:N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

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Chemical Property of N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

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Technology Process of N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

There total 4 articles about N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

N-phenyl-2,4-dinitro-benzenesulfonamide: 38225-88-6
N-phenyl-2,4-dinitro-benzenesulfonamide

: N-benzyl-N-(3-hydroxypropyl)-2,4-dinitrobenzenesulfonamide

: 1606142-75-9
N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 100-39-0
benzyl bromide

: 1606142-75-9
N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; 2: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 1606142-75-9
N-benzyl-N-(3-(2,4-dinitro-(N-phenyl) phenylsulfonamido)propyl)-2,4 dinitro benzene sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -78 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046