(S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Base Information

• Chemical Name: (S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide
• CAS No.: 121451-41-0
• Molecular Formula: C₂₄H₂₈N₂O₄S₂
• Molecular Weight: 472.629

Synonyms:(S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Chemical Property of (S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

Chemical Property:

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Technology Process of (S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

There total 1 articles about (S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,2'-dithiodibenzoic acid dichloride (19602-82-5) + (S)-1-Pyrrolidin-2-yl-methanol (23356-96-9) → (S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide (121451-41-0)

Guidance literature:

With triethylamine; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1002/jhet.5570250358

Reference yield: 98.0%

(S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide (121451-41-0) → (S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide (121451-45-4)

Guidance literature:

With thionyl chloride; air; In chloroform; for 2h; Heating; room temperature 1 h, then reflux 2 h;

DOI:10.1002/jhet.5570250358

Reference yield: 95.0%

(S)-bis<2-<<2-(hydroxymethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide (121451-41-0) → N-(2-mercaptobenzoyl)-L-prolinol (121451-42-1)

Guidance literature:

With sodium dithionite; sodium carbonate; In water; for 0.75h; Heating;

DOI:10.1002/jhet.5570250358

upstream raw materials:

2,2'-dithiodibenzoic acid dichloride

(S)-1-Pyrrolidin-2-yl-methanol

Downstream raw materials:

N-(2-mercaptobenzoyl)-L-prolinol

(S)-bis<2-<<2-(chloromethyl)-1-pyrrolidinyl>carbonyl>phenyl> disulphide

(S)-N-(2-mercaptobenzoyl)-2-(chloromethyl)pyrrolidine

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