Technology Process of C28H25F5O7S2
There total 6 articles about C28H25F5O7S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 11 steps
1: potassium carbonate / tetrahydrofuran
2: lithium aluminium tetrahydride / tetrahydrofuran
3: potassium tert-butylate / tetrahydrofuran
4: Dess-Martin periodane / dichloromethane
5: trimethylsilyl trifluoromethanesulfonate
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane
7: boron trifluoride diethyl etherate / dichloromethane
8: triethylamine / dichloromethane
9: potassium tert-butylate / tetrahydrofuran
10: ozone / dichloromethane
11: triethylamine
With
lithium aluminium tetrahydride; trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate; potassium tert-butylate; potassium carbonate; Dess-Martin periodane; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
1: |Michael Addition;
DOI:10.1016/j.bmcl.2012.11.047
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane
2: boron trifluoride diethyl etherate / dichloromethane
3: triethylamine / dichloromethane
4: potassium tert-butylate / tetrahydrofuran
5: ozone / dichloromethane
6: triethylamine
With
boron trifluoride diethyl etherate; potassium tert-butylate; ozone; triethylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.11.047
