C₂₃H₁₈N₂O₆

Base Information

• Chemical Name: C₂₃H₁₈N₂O₆
• CAS No.: 1380109-94-3
• Molecular Formula: C₂₃H₁₈N₂O₆
• Molecular Weight: 418.406
• Mol file: 1380109-94-3.mol

Synonyms:C₂₃H₁₈N₂O₆

Chemical Property of C₂₃H₁₈N₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₁₈N₂O₆

There total 5 articles about C₂₃H₁₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl 4,5-bis(benzyloxy)picolinate (112334-42-6) → C23H18N2O6 (1380109-94-3)

Guidance literature:

Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / ethanol / 0.33 h / 0 - 20 °C / Enzymatic reaction

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 65 °C

3.1: hydroxylamine hydrochloride; sodium acetate / methanol / 3 h / Reflux

4.1: N-chloro-succinimide; pyridine / tetrahydrofuran / 0.5 h / 55 °C

4.2: 0 °C / Inert atmosphere

4.3: 0.75 h / 5 °C / Inert atmosphere

5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C

6.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

With pyridine; sodium tetrahydroborate; N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; 3-chloro-benzenecarboperoxoic acid; lithium hydroxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetonitrile;

DOI:10.1021/jm400560z

Reference yield:

C20H18N2O3 (1380109-90-9) → C23H18N2O6 (1380109-94-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-chloro-succinimide; pyridine / tetrahydrofuran / 0.5 h / 55 °C

1.2: 0 °C / Inert atmosphere

1.3: 0.75 h / 5 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C

3.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

With pyridine; N-chloro-succinimide; 3-chloro-benzenecarboperoxoic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1021/jm400560z

Reference yield:

C24H20N2O5 (1380109-91-0) → C23H18N2O6 (1380109-94-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C

2: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

With 3-chloro-benzenecarboperoxoic acid; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1021/jm400560z

upstream raw materials:

benzyl 4,5-bis(benzyloxy)picolinate

4,5-bis(phenylmethoxy)-2-pyridinemethanol

C₂₀H₁₈N₂O₃

C₂₄H₂₀N₂O₅

Downstream raw materials:

C₄₅H₅₀N₈O₁₂S

C₄₅H₅₀N₈O₁₅S₂