Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

Base Information

Chemical Name:Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate
CAS No.:944445-72-1
Molecular Formula:C₂₇H₂₃N₃O₆
Molecular Weight:485.496
Hs Code.:

Synonyms:Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

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Chemical Property of Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

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Technology Process of Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

There total 1 articles about Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 944445-73-2
methyl 2-amino-5-[(1-amino-2-methylindolizin-3-yl)carbonyl]benzoate

: 6304-89-8
3-acetoxybenzoic acid

: 944445-72-1
Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

Guidance literature:: 3-acetoxybenzoic acid; With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

methyl 2-amino-5-[(1-amino-2-methylindolizin-3-yl)carbonyl]benzoate; In N,N-dimethyl-formamide; for 16h;

Reference yield: 84.0%

: 944445-72-1
Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

: 944445-74-3
Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

Guidance literature:: Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate; With water; potassium carbonate; In methanol; at 20 ℃; for 1h;

With hydrogenchloride; In methanol; water; ethyl acetate;