Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

Base Information

Chemical Name:Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate
CAS No.:944445-74-3
Molecular Formula:C₂₅H₂₁N₃O₅
Molecular Weight:443.459
Hs Code.:

Synonyms:Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

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Chemical Property of Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

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Technology Process of Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

There total 1 articles about Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 944445-72-1
Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate

: 944445-74-3
Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

Guidance literature:: Methyl 5-[(1-{[3-(acetyloxy)benzoyl]amino}-2-methylindolizin-3-yl)-carbonyl]-2-aminobenzoate; With water; potassium carbonate; In methanol; at 20 ℃; for 1h;

With hydrogenchloride; In methanol; water; ethyl acetate;

Reference yield: 76.0%

: 927-68-4
bromoethyl acetate

: 944445-74-3
Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

: C₂₉H₂₇N₃O₇

Guidance literature:: Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

bromoethyl acetate; In N,N-dimethyl-formamide; at 70 ℃; for 1h;

With hydrogenchloride; water; In N,N-dimethyl-formamide;

Reference yield: 61.0%

: 24772-63-2
1,8-diiodooctane

: 944445-74-3
Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate

: 944445-75-4
3,3'-{octane-1,8-diylbis[oxy-3,1-phenylenecarbonylimino(2-methylindolizine-1,3-diyl)carbonyl]}bis(methyl 6-aminobenzoate)

Guidance literature:: Methyl 2-amino-5-({1-[(3-hydroxybenzoyl)-amino]-2-methylindolizin-3-yl}carbonyl)benzoate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

1,8-diiodooctane; In N,N-dimethyl-formamide; at 60 ℃; for 72h;

With potassium hydrogensulfate; water; In N,N-dimethyl-formamide;