3-(2-{2-[2-(3-Formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde

Base Information

• Chemical Name: 3-(2-{2-[2-(3-Formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde
• CAS No.: 115142-66-0
• Molecular Formula: C₂₀H₂₂O₈
• Molecular Weight: 390.39
• European Community (EC) Number: 856-987-0
• Nikkaji Number: J697.411B

Synonyms:115142-66-0;3-(2-{2-[2-(3-formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde;3-[2-[2-[2-(3-Formyl-2-hydroxy-phenoxy)ethoxy]ethoxy]ethoxy]-2-hydroxybenZaldehyde;3-(2-(2-[2-(3-FORMYL-2-HYDROXYPHENOXY)ETHOXY]ETHOXY)ETHOXY)-2-HYDROXYBENZALDEHYDE;SCHEMBL24189814;MFCD22194423;AKOS040767989;CS-0241351;G54791;EN300-23254233;3,3'-(3,6-dioxaoctane-1,8-diyldioxy)-bis(2-hydroxybenzaldehyde);3,3'-(((Ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2-hydroxybenzaldehyde)

Chemical Property of 3-(2-{2-[2-(3-Formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 13
• Exact Mass: 390.13146766
• Heavy Atom Count: 28
• Complexity: 406

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)OCCOCCOCCOC2=CC=CC(=C2O)C=O)O)C=O

Technology Process of 3-(2-{2-[2-(3-Formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde

There total 1 articles about 3-(2-{2-[2-(3-Formyl-2-hydroxyphenoxy)ethoxy]ethoxy}ethoxy)-2-hydroxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2,3-dihydroxybenzaldehyde (24677-78-9) + triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 3,3'-(((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2-hydroxybenzaldehyde) (115142-66-0)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; 1.) 1 h; 2.) 24 h;

DOI:10.1021/ja00223a017

Reference yield: 80.0%

1,1'-dimethyl-P-phenyl-phosphonic-dihydrazide (54529-67-8) + barium trifluoromethanesulfonate (2794-60-7) + 3,3'-(((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2-hydroxybenzaldehyde) (115142-66-0) → C28H33N4O7P*2CF3O3S(1-)*Ba(2+)

Guidance literature:

In methanol; for 3h; Heating;

DOI:10.1021/ja00111a007

Reference yield: 77.0%

N-methoxylamine hydrochloride (593-56-6) + 3,3'-(((ethane-1,2-diylbis(oxy))bis(ethane-2,1-diyl))bis(oxy))bis(2-hydroxybenzaldehyde) (115142-66-0) → 3,3'-<1,2-ethanediylbis(oxy-2,1-ethanediyloxy)>bis(2-hydroxybenzaldehyde) bis(O-methyloxime) (119638-40-3)

Guidance literature:

With sodium carbonate; In methanol; water; at 50 ℃; for 0.5h;

DOI:10.1021/jo00271a021

upstream raw materials:

2,3-dihydroxybenzaldehyde

triethylene glycol di-(p-toluenesulfonate)

Downstream raw materials:

3,3'-<1,2-ethanediylbis(oxy-2,1-ethanediyloxy)>bis(2-hydroxybenzaldehyde) bis(O-methyloxime)

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