4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Base Information

Chemical Name:4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide
CAS No.:176512-24-6
Molecular Formula:C₂₁H₂₀N₂O₄S₂
Molecular Weight:428.533
Hs Code.:

Synonyms:4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Suppliers and Price of 4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Chemical Property:

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Technology Process of 4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

There total 1 articles about 4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 3-Methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenylamine

: 176512-24-6
4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

Guidance literature:: In pyridine; for 3h; Yield given;
DOI:10.1002/ardp.19963290309

Reference yield: 60.0%

: 176512-24-6
4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

: 176512-33-7
2,2'-dimethyl-4-N-tosylamino-4'-nitrodiphenyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 24h;
DOI:10.1002/ardp.19963290309

Reference yield:

: 176512-24-6
4-Methyl-N-[3-methyl-4-(2-methyl-4-nitro-phenylsulfanyl)-phenyl]-benzenesulfonamide

: 35880-74-1
4,4'-diamino-2,2'-dimethyldiphenyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 90percent MCPBA / CHCl₃ / 24 h

2: 92 percent / conc. H₂SO₄

3: 96 percent / H₂ / 10percent Pd/C / acetic acid

With sulfuric acid; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In chloroform; acetic acid;
DOI:10.1002/ardp.19963290309