C₆₁H₁₀₀O₈Si₃

Base Information

Chemical Name:C₆₁H₁₀₀O₈Si₃
CAS No.:1160221-76-0
Molecular Formula:C₆₁H₁₀₀O₈Si₃
Molecular Weight:1045.72
Hs Code.:

C<sub>61</sub>H<sub>100</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₆₁H₁₀₀O₈Si₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₁H₁₀₀O₈Si₃

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Technology Process of C₆₁H₁₀₀O₈Si₃

There total 26 articles about C₆₁H₁₀₀O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₇H₁₀₈O₈SeSi₃

: 1160221-76-0
C₆₁H₁₀₀O₈Si₃

Guidance literature:: With water; dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; at 30 ℃; for 21h;
DOI:10.1021/ol900769d

Reference yield:

: C₆₇H₁₀₆O₈SeSi₃

: 1160221-76-0
C₆₁H₁₀₀O₈Si₃

Guidance literature:: With dihydrogen peroxide; sodium hydrogencarbonate; In tetrahydrofuran; at 20 - 30 ℃;
DOI:10.1016/j.tet.2010.05.069

Reference yield:

: 924656-53-1
C₆₅H₁₀₄O₉Si₃

: 1160221-76-0
C₆₁H₁₀₀O₈Si₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4,4'-di-tert-butylbiphenyl; lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

3.2: -78 - 20 °C / Inert atmosphere

4.1: dihydrogen peroxide; sodium hydrogencarbonate / tetrahydrofuran; water / 21 h / 30 °C

With 4,4'-di-tert-butylbiphenyl; dihydrogen peroxide; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; lithium; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; 2.1: Parikh-Doering oxidation / 3.1: Wittig reaction / 3.2: Wittig reaction;
DOI:10.1021/ja200089f