ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

Base Information

Chemical Name:ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate
CAS No.:79938-13-9
Molecular Formula:C₁₉H₁₇ClFNO₅
Molecular Weight:393.799
Hs Code.:

Synonyms:ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

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Chemical Property of ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

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Technology Process of ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

There total 7 articles about ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105-36-2
ethyl bromoacetate

: 79938-12-8
7-chloro-3-(2-fluoro-4-ethoxyphenyl)-6-hydroxy-1,2-benzisoxazole

: 79938-13-9
ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 65 ℃; for 1h; Yield given;
DOI:10.1021/jm00343a008

Reference yield:

: 458-03-7
1-ethoxy-3-fluorobenzene

: 79938-13-9
ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / AlCl₃ / 1,2-dichloro-ethane / 2 h / 5 °C

2: hydroxylamine hydrochloride, pyridine / 24 h / Heating

3: 89 percent / sodium hydride / dimethylformamide / 0.5 h / Ambient temperature

4: 65.5 percent / pyridine hydrochloride / 2 h / 180 °C

5: K₂CO₃ / dimethylformamide / 1 h / 65 °C

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; pyridine hydrochloride; sodium hydride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00343a008

Reference yield:

: 76238-31-8
2,3-dichloro-4-methoxybenzoyl chloride

: 79938-13-9
ethyl <<7-chloro-3-(2-fluoro-4-ethoxyphenyl)-1,2-benzisoxazol-6-yl>oxy>acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 30 percent / AlCl₃ / 1,2-dichloro-ethane / 2 h / 5 °C

2: hydroxylamine hydrochloride, pyridine / 24 h / Heating

3: 89 percent / sodium hydride / dimethylformamide / 0.5 h / Ambient temperature

4: 65.5 percent / pyridine hydrochloride / 2 h / 180 °C

5: K₂CO₃ / dimethylformamide / 1 h / 65 °C

With pyridine; aluminium trichloride; hydroxylamine hydrochloride; pyridine hydrochloride; sodium hydride; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00343a008