Co₂(CO)6(C₆H₅CCCH₂OH)

Base Information

Chemical Name:Co₂(CO)6(C₆H₅CCCH₂OH)
CAS No.:163461-71-0
Molecular Formula:C₁₅H₈Co₂O₇
Molecular Weight:418.211
Hs Code.:

Co<sub>2</sub>(CO)6(C<sub>6</sub>H<sub>5</sub>CCCH<sub>2</sub>OH)

Synonyms:Co₂(CO)6(C₆H₅CCCH₂OH)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Co₂(CO)6(C₆H₅CCCH₂OH)

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Technology Process of Co₂(CO)6(C₆H₅CCCH₂OH)

There total 2 articles about Co₂(CO)6(C₆H₅CCCH₂OH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 90108-98-8
μ-η2-(3-phenyl-2-propynal)dicobalthexacarbonyl

: ((C₆H₅CCCHOH)Co₂(CO)6)2

: 163461-71-0
Co₂(CO)6(C₆H₅CCCH₂OH)

Guidance literature:: With Mn; Cp₂TiCl₂; Me₃SiCl; In tetrahydrofuran; under N2 atm. Mn and Co2TiCl2 in THF were stirred for 20min, Me3SiCl wasadded, soln. (phenylpropynal)dicobalt hexacarbonyl in THF was added and stirred for 4 h; soln. was filtered and purified by TLC (petroleum ether-ether 97:3);
DOI:10.1021/om030392t

Reference yield:

: 15226-74-1,61091-28-9,61117-58-6
dicobalt octacarbonyl

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 163461-71-0
Co₂(CO)6(C₆H₅CCCH₂OH)

Guidance literature:: In dichloromethane; under inert atm.; stirred; addn. of Co2(CO)8 portionwise; stirred for 7h; removed solvent; stored at -25°C;