C₁₀H₇ClO₂

Base Information

• Chemical Name: C₁₀H₇ClO₂
• CAS No.: 1174508-79-2
• Molecular Formula: C₁₀H₇ClO₂
• Molecular Weight: 194.617

Synonyms:C₁₀H₇ClO₂

Chemical Property of C₁₀H₇ClO₂

Chemical Property:

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Technology Process of C₁₀H₇ClO₂

There total 1 articles about C₁₀H₇ClO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propargyl alcohol (107-19-7) + 2-bromo-4-chlorobenzaldehyde (84459-33-6) → C10H7ClO2 (1174508-79-2)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; at 50 ℃; Inert atmosphere;

DOI:10.1002/chem.201900890

Reference yield: 62.0%

2,3-dihydro-3-keto-5-chlorobenzothiophene (51942-80-4) + C10H7ClO2 (1174508-79-2) → (Z)-5-chloro-2-(4-chloro-2-(3-hydroxyprop-1-yn-1-yl)benzylidene)benzo[b]thiophen-3(2H)-one

Guidance literature:

With piperidine; In toluene; at 85 ℃; for 4h; Inert atmosphere;

DOI:10.1002/chem.201900890

Reference yield:

C10H7ClO2 (1174508-79-2) + chloroformic acid ethyl ester (541-41-3) → C13H11ClO4 (1174508-34-9)

Guidance literature:

With pyridine; 2,2-bis(hydroxymethyl)propionic acid; In dichloromethane; at 0 - 20 ℃; for 2h;

DOI:10.1021/ol901265b

upstream raw materials:

propargyl alcohol

2-bromo-4-chlorobenzaldehyde

Downstream raw materials:

C₁₂H₉ClO₃

C₁₃H₁₁ClO₄

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