6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

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Chemical Name:6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester
CAS No.:228710-74-5
Molecular Formula:C₂₉H₃₇N₅O₆S
Molecular Weight:583.709
Hs Code.:

Synonyms:6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

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Chemical Property of 6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

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Technology Process of 6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

There total 3 articles about 6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 228710-73-4
6-Chlorosulfonyl-chroman-(2S)-carboxylic acid isobutyl ester

: 182251-91-8
1-(4-aminophenyl)-4-(3-cyclopentylpropyl)-5-tetrazolone

: 228710-74-5
6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

Guidance literature:: With pyridine; dmap; In tetrahydrofuran; at 60 ℃; for 16h;

Reference yield:

: (2S)-Chromancarboxylic acid isobutyl ester

: 228710-74-5
6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 1,1-dichloroethane

2: pyridine; dmap / tetrahydrofuran; hexane; dichloromethane

With pyridine; chlorosulfonic acid; dmap; In tetrahydrofuran; 1,1-dichloroethane; hexane; dichloromethane;

Reference yield:

: 83780-46-5
(2S)-3,4-dihydro-2H-chromene-2-carboxylic acid

: 228710-74-5
6-{4-[4-(3-Cyclopentyl-propyl)-5-oxo-4,5-dihydro-tetrazol-1-yl]-phenylsulfamoyl}-chroman-(2S)-carboxylic acid isobutyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N-methyl-acetamide

2: chlorosulfonic acid / 1,1-dichloroethane

3: pyridine; dmap / tetrahydrofuran; hexane; dichloromethane

With pyridine; chlorosulfonic acid; dmap; caesium carbonate; In tetrahydrofuran; N-methyl-acetamide; 1,1-dichloroethane; hexane; dichloromethane;