(2,4,6-trinitrophenyl)acetic acid

Base Information

• Chemical Name: (2,4,6-trinitrophenyl)acetic acid
• CAS No.: 77601-83-3
• Molecular Formula: C8H5N3O8
• Molecular Weight: 271.143

Synonyms:

Chemical Property of (2,4,6-trinitrophenyl)acetic acid

Chemical Property:

• Vapor Pressure: 4.79E-09mmHg at 25°C
• Boiling Point: 454.3°Cat760mmHg
• Flash Point: 198.7°C
• Density: 1.779g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,4,6-trinitrophenyl)acetic acid

There total 7 articles about (2,4,6-trinitrophenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

β-(2,4,6-trinitrophenyl)ethanol (2290-14-4) → 2,4,6-trinitrophenylacetic acid (77601-83-3)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; at 50 - 80 ℃; for 3h;

DOI:10.1021/jo000479d

Reference yield: 72.0%

acetic acid-(2,4,6-trinitro-phenethyl ester) (90946-97-7) → 2,4,6-trinitrophenylacetic acid (77601-83-3)

Guidance literature:

With chromium(VI) oxide; sulfuric acid;

DOI:10.1081/SCC-120002132

Reference yield:

→ 2,4,6-trinitrophenylacetic acid (77601-83-3)

Guidance literature:

With sulfuric acid;

upstream raw materials:

picryl-malonic acid diethyl ester

sulfuric acid

β-(2,4,6-trinitrophenyl)ethanol

acetic acid-(2,4,6-trinitro-phenethyl ester)

Downstream raw materials:

3-(2,4,6-Trinitrostyryl)-pyren

2,4,6-Trinitro-2',4',6'-trimethoxystilben

2,4,6-Trinitrotoluene

carbon dioxide

Refernces

Synthesis of 1-aryl-4,6-dinitro-1H-indazoyl-3-methylcarboxylates

10.1081/SCC-120002132

The study focuses on the synthesis of 1-aryl-4,6-dinitro-1H-indazoyl-3-methylcarboxylates, which are derived from 2,4,6-trinitrotoluene (TNT) derivatives. The researchers aimed to modify the 4,6-dinitroindazole structure by introducing a new substituent, leading to the development of a facile method for synthesizing methyl esters of 1-aryl-4,6-dinitro-1H-indazolyl-3-carboxylic acids. Key chemicals used in the study include TNT, which was converted into 2,4,6-trinitrophenylacetic acid, and then into methyl picrylacetate. Diazonium salts were reacted with this ester to form hydrazones, which underwent cyclization to yield the desired indazoles. The purpose of these chemicals was to facilitate the synthesis of new indazole derivatives, which were obtained in good yields and had their structures confirmed through microanalyses and NMR spectra.

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